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Facilities |
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TEM |
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SESAM
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JEOL ARM 1250 KV
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JEOL 4000FX
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Philips CM200
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HRTEM (Scherzer resolution) |
0.24 nm |
0.12 nm |
0.2 nm |
0.27 nm |
X-ray analysis (spatial resolution) |
1 nm |
– |
>20 nm |
– |
EELS analysis spatial resolution energy resolution |
parallel >0.5 nm 0.1–0.2 eV |
parallel >20 nm ≥1 eV |
– |
– |
| Maximal tilt angle |
30°/15° |
45°/45° |
30°/15° |
60°/30° |
Heating stage (max. temperature) |
900 °C |
900 °C |
900 °C |
– |
| Cooling stage |
–160 °C |
–160 °C |
–160 °C |
–160 °C |
| Deformation stage |
– |
– |
– |
– |
| Energy-filtering TEM |
yes |
yes |
– |
yes |
| Z-contrast |
yes |
– |
– |
– |
Orientation measurements by Kikuchi patterns |
– |
– |
– |
– |
| Energy-filtered diffraction |
yes large angle |
– |
– |
yes |
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TEM (continued) |
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ZEISS 912 Omega
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VG HB 501UX
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HRTEM (Scherzer resolution) |
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– |
– |
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X-ray analysis (spatial resolution) |
|
>20 nm |
1 nm |
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EELS analysis spatial resolution energy resolution |
|
parallel >20 nm 0.9 eV |
parallel >0.5 nm 0.3–0.7 eV |
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| Maximal tilt angle |
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60°/30° |
10°/10° |
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Heating stage (max. temperature) |
|
900 °C |
– |
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| Cooling stage |
|
–160 °C |
– |
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| Deformation stage |
|
– |
– |
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| Energy-filtering TEM |
|
yes |
– |
|
| Z-contrast |
|
– |
yes |
|
| Orientation measurements by Kikuchi patterns |
|
yes |
– |
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| Energy-filtered diffraction |
|
yes limited angle |
– |
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SEM |
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LEO 438VP
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JSM 6300F
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JEM 6400
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EPMA
Cameca SX 100
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| Resolution |
5 nm |
3 nm |
5 nm |
6 nm |
| Tilt angle |
90° |
15° |
(15°) |
– |
| EDS |
yes |
yes |
yes |
(yes) |
| BSE |
yes |
yes |
yes |
yes |
| OIM |
yes |
– |
– |
– |
| WDS |
– |
– |
yes |
yes |
| Spectrometer |
– |
– |
2 |
5 |
| Crystals |
– |
– |
LIF, PET, TAP STE |
LIF, PET, TAP PC0, PC1, PC2, PC3 |
| Large Crystals |
– |
– |
– |
LLIF, LPET LPC1, LPC2 |
Anticontamination equipment |
– |
– |
– |
air jet, cooling plate |
| Pump system (EPMA) |
– |
– |
turbo pump |
turbo pump, oil free primary pump |
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